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Analytical and Lab

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Instrumentation and Standard Services

The KGS laboratory specializes in environmental analysis of:

  • Water quality and contamination
  • Coal quality and composition
  • Rocks and minerals
  • Other natural resources
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About the KGS Laboratory

This service is provided primarily to researchers at KGS, but also to representatives of academia, government, industry, and the private sector who study the environment and natural resources of Kentucky. As part of our mission to serve the public, we require that results of analyses run for non-KGS researchers enhance our publicly available databases.

 

We offer trained professional staff and state-of-the-art automated equipment, and use the latest techniques to efficiently analyze samples. Our goal is to provide quality and timely analytical service to meet any specific requirements. We also train UK students in the principles and practice of various analytical techniques and instruments, including total organic carbon, X-ray diffraction, and X-ray fluorescence. Graduate students from a wide range of studies use the lab facilities and experience of the lab personnel.

 

KGS uses a laboratory information management system to track sample status from log-in to final reporting. This LIMS technology is based on current EPA recommendations for ensuring data integrity in an automated laboratory operation. We also provide electronic data transfer using various types of media and database formats.

X-Ray Diffraction Instrument Scheduling

To reserve time on the XRD instrument located in room 369 of the Mining and Mineral Resources Building:

  1. First follow the XRD schedule link and locate an unscheduled time you wish to reserve.
  2. Second, send an email with the date and time, and we will update the schedule to indicate your reservation.
  3. If you need to cancel your scheduled time, please do so as soon as possible.
  4. Please direct questions regarding X-ray diffraction scheduling to: Jason Backus
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EVA Introduction Help File

An introductory help file on the utilization of the XRD scan evaluation software - EVA

View Help File (PDF) →
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Analytical Geochemistry Services Fact Sheet

Complete overview of analytical geochemistry laboratory capabilities

Download Fact Sheet (PDF) →
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X-ray Diffraction Operating Procedures

Guidelines for proper XRD instrument operation and safety

View Procedures (PDF) →
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University of Kentucky Radiation Safety

UK safety requirements and training for X-ray equipment

Safety Info (PDF) →

Laboratory Services by Category

๐Ÿงช Metals Analysis

Inductively coupled argon plasma spectrometry (ICAP)

Total & dissolved metals analysis:

Al, Sb, As, Ba, Be, B, Cd, Ca, Cr, Co, Cu, Au, Fe, Pb, Li, Mg, Mn, Ni, P, K, Se, Si, Ag, Na, Sr, S, Tl, Sn, V, Zn

Method: EPA 200.7A, SW846 (series 6000)

๐Ÿ’Ž Mineralogy

  • X-ray diffraction spectrometry (XRD)
  • X-ray fluorescence spectrometry (XRF)
  • Major and minor elements analysis
  • Complete mineralogical identification

๐Ÿ’ง Water Parameters

Analytical Methods:

  • UV-visible spectrometry
  • Ion chromatography
  • Conductance measurement
  • Classical wet chemistry

Key Parameters:

  • pH, alkalinity, hardness
  • Nutrients (N, P compounds)
  • Major ions (Clโป, SOโ‚„²โป, etc.)
  • Organic contaminants

โšซ Coal Quality

  • Proximate analysis (moisture, ash, volatile matter, fixed carbon)
  • Total sulfur content
  • Calorific value determination
  • Ash mineral analysis

Quality Assurance and Quality Control

The KGS laboratory maintains a quality-control program to assure reliable results. This comprehensive program provides the highest confidence in precision as well as in accuracy for all our analyses. All analytical instruments are calibrated regularly, and complete calibration records are maintained.

 

Results accuracy are verified using certified calibration standards, traceable to National Institute of Standards and Technology and American Association for Laboratory Accreditation sources when possible.

 

In an effort to continually improve the quality of our service, we have adopted an intralaboratory performance testing program. We participate in intralabratory proficiency testing programs offered by the U.S. Geological Survey, Quality Assurance Resources, Quality Associates International Ltd., and Analytical Geochemistry Laboratories.

 

Each test method follows established quality-control measures that are clearly defined in all standard operation procedures. These SOPs, as well as the laboratory quality-assurance plan, may be reviewed by interested parties. A written summary of all quality-control data associated with a group of samples will be made available upon request.

Proficiency Testing

We participate in proficiency testing programs offered by:

  • U.S. Geological Survey
  • Quality Assurance Resources
  • Quality Associates International Ltd.
  • Analytical Geochemistry Laboratories

Laboratory Gallery

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Wet chemistry/nutrient testing using an HACH analyzer.

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Total dissolved solids testing.

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Coal quality lab with proximate, calorimeter, and carbon/sulfur analyzer.

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Proximate analyzer used in coal-quality analysis.

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Graduate student from the University of Kentucky using X-ray diffraction.

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X-ray fluorescence sample preparation using an automated fluxer.

Laboratory Contact

For current information about analytical services from KGS Laboratory Services:

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Important Note

Lab analysis services may change over time. Please contact us for current service availability and pricing.

Detailed Service Information

For a complete list of analytical parameters and methods, visit our detailed services page.

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Research Team

Analytical Chemistry Laboratory

Team Leader

Jason Backus

Jason Backus

Team Lead

Laboratory Manager

jbackus@uky.edu

๐Ÿ“ž 859-323-0555

Core KGS Team Members